Information card for entry 7132846

Structure parameters

• Formula: C73 H110 N10 Ni2 P4 Sc2
• Calculated formula: C73 H110 N10 Ni2 P4 Sc2
• Title of publication: A scandium metalloligand supported Ni(0) complex with a heterobimetallocycle: versatile reactivity with unsaturated bonds.
• Authors of publication: Ma, Lei; Pan, Xiaowei; Hong, Dongjing; Fang, Huayi; Cui, Peng
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 31
• Pages of publication: 4222 - 4225
• a: 12.49 ± 0.006 Å
• b: 12.54 ± 0.006 Å
• c: 13.517 ± 0.006 Å
• α: 65.861 ± 0.006°
• β: 73.439 ± 0.006°
• γ: 76.945 ± 0.006°
• Cell volume: 1837.3 ± 1.5 ų
• Cell temperature: 293.15 K
• Ambient diffraction temperature: 293.15 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0741
• Residual factor for significantly intense reflections: 0.0452
• Weighted residual factors for significantly intense reflections: 0.1038
• Weighted residual factors for all reflections included in the refinement: 0.1138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No