Information card for entry 7132891
| Formula |
C32 H42 N2 O4 |
| Calculated formula |
C32 H42 N2 O4 |
| Title of publication |
Stereocontrol in an intermolecular Schmidt reaction of equilibrating hydroxyalkyl allylic azides. |
| Authors of publication |
Liu, Ruzhang; Wang, Juan; Wu, Hao; Quan, Xianfeng; Wang, Shilin; Guo, Jiandong; Wang, Yang; Li, Heting |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2024 |
| Journal volume |
60 |
| Journal issue |
32 |
| Pages of publication |
4362 - 4365 |
| a |
5.6228 ± 0.0006 Å |
| b |
11.5801 ± 0.0011 Å |
| c |
22.772 ± 0.002 Å |
| α |
88.886 ± 0.003° |
| β |
84.246 ± 0.003° |
| γ |
83.434 ± 0.003° |
| Cell volume |
1465.5 ± 0.2 Å3 |
| Cell temperature |
296 K |
| Ambient diffraction temperature |
296 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.1905 |
| Residual factor for significantly intense reflections |
0.0987 |
| Weighted residual factors for significantly intense reflections |
0.2986 |
| Weighted residual factors for all reflections included in the refinement |
0.3473 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.048 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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https://www.crystallography.net/7132891.html
