Information card for entry 7132921

Structure parameters

• Formula: C67 H25 Al As2 Cl2 Cu F46 Mo4 N O11 Sb2
• Calculated formula: C67 H25 Al As2 Cl2 Cu F46 Mo4 N O11 Sb2
• Title of publication: Supramolecular compounds assembled from the heteroleptic tetrahedral complex [{CpMo(CO)₂}₂(μ,η²-AsSb)] and metal salts.
• Authors of publication: Elsayed Moussa, Mehdi; Shelyganov, Pavel A.; Seidl, Michael; Zimmermann, Lisa; Scheer, Manfred
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 35
• Pages of publication: 4703 - 4706
• a: 20.9582 ± 0.0002 Å
• b: 33.303 ± 0.0004 Å
• c: 12.1289 ± 0.0002 Å
• α: 90°
• β: 105.237 ± 0.001°
• γ: 90°
• Cell volume: 8168.03 ± 0.19 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 11
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.0467
• Weighted residual factors for significantly intense reflections: 0.1231
• Weighted residual factors for all reflections included in the refinement: 0.1255
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No