Information card for entry 7132944

Structure parameters

• Formula: C100 H86 N2 O32 P4 W10
• Calculated formula: C100 H86 N2 O32 P4 W10
• Title of publication: Photocatalytic aerobic α-oxygenation of amides to imides using a highly durable decatungstate tetraphenylphosphonium salt.
• Authors of publication: Gu, Chen; Yatabe, Takafumi; Yamaguchi, Kazuya; Suzuki, Kosuke
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 37
• Pages of publication: 4906 - 4909
• a: 13.5793 ± 0.0002 Å
• b: 15.3135 ± 0.0003 Å
• c: 15.4699 ± 0.0002 Å
• α: 117.216 ± 0.0016°
• β: 113.848 ± 0.0016°
• γ: 92.658 ± 0.0014°
• Cell volume: 2508.49 ± 0.1 ų
• Cell temperature: 93.15 K
• Ambient diffraction temperature: 93.15 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0514
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.0806
• Weighted residual factors for all reflections included in the refinement: 0.0857
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No