Information card for entry 7133122

Structure parameters

• Formula: C85.6 H117 Cl La N2 O1.9 P2
• Calculated formula: C84 H113 Cl La N2 O1.5 P2
• Title of publication: A bridging bis-phosphanido-phosphinidene complex of lanthanum supported by a sterically encumbering PN ligand.
• Authors of publication: Wittwer, B.; Heim, F.; Wurst, K.; Hohloch, S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 57
• Pages of publication: 7299 - 7302
• a: 20.5986 ± 0.0013 Å
• b: 24.7411 ± 0.0015 Å
• c: 32.569 ± 0.002 Å
• α: 90°
• β: 95.767 ± 0.002°
• γ: 90°
• Cell volume: 16514.2 ± 1.8 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0703
• Residual factor for significantly intense reflections: 0.0519
• Weighted residual factors for significantly intense reflections: 0.1159
• Weighted residual factors for all reflections included in the refinement: 0.1299
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No