Information card for entry 7133126

Structure parameters

• Formula: C27 H23 F Ge O
• Calculated formula: C27 H23 F Ge O
• Title of publication: Photoinduced decarboxylative germylation of α-fluoroacrylic acids: access to germylated monofluoroalkenes.
• Authors of publication: Lu, Xiao-Yu; Qian, Yu-Jun; Sun, Hai-Lun; Su, Meng-Xue; Wang, Zi-Zhen; Jiang, Fan; Zhou, Xin-Yue; Sun, Yan-Xi; Shi, Wan-Li; Wan, Ji-Ru
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 51
• Pages of publication: 6556 - 6559
• a: 9.8789 ± 0.0001 Å
• b: 11.0575 ± 0.0002 Å
• c: 11.8202 ± 0.0002 Å
• α: 106.201 ± 0.001°
• β: 104.242 ± 0.001°
• γ: 105.035 ± 0.001°
• Cell volume: 1124.69 ± 0.03 ų
• Cell temperature: 170 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0356
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0902
• Weighted residual factors for all reflections included in the refinement: 0.0914
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No