Information card for entry 7133344

Structure parameters

• Formula: C34.06 H68.23 N4 O0.06 S2 Si4 Yb
• Calculated formula: C34 H68 N4 S2 Si4 Yb
• Title of publication: Yb/Si frustrated Lewis pairs with a labile naphthalenyl bridge.
• Authors of publication: Xu, Cheng; Zhao, Sixuan; Zhang, Heng; Peng, Qian; Chen, Yaofeng
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 64
• Pages of publication: 8411 - 8414
• a: 15.4962 ± 0.0003 Å
• b: 17.7037 ± 0.0003 Å
• c: 19.308 ± 0.0003 Å
• α: 78.382 ± 0.001°
• β: 69.436 ± 0.001°
• γ: 69.691 ± 0.002°
• Cell volume: 4632.04 ± 0.15 ų
• Cell temperature: 173 ± 0.1 K
• Ambient diffraction temperature: 173 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0499
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.0793
• Weighted residual factors for all reflections included in the refinement: 0.0844
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No