Information card for entry 7133439

Structure parameters

• Formula: C22 H15 F N2
• Calculated formula: C22 H15 F N2
• Title of publication: Synthesis of polysubstituted pyridazines <i>via</i> Cu-mediated C(sp³)-C(sp³) coupling/annulation of saturated ketones with acylhydrazones.
• Authors of publication: Zhou, Honggui; Li, Zhefeng; Chen, Juehong; Zhou, Si; Wang, Xinyu; Zhang, Linwei; Chen, Jiuxi; Lv, Ningning
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 71
• Pages of publication: 9546 - 9549
• a: 8.757 ± 0.004 Å
• b: 9.973 ± 0.004 Å
• c: 11.506 ± 0.004 Å
• α: 103.314 ± 0.011°
• β: 100.861 ± 0.012°
• γ: 113.664 ± 0.011°
• Cell volume: 850 ± 0.6 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0952
• Residual factor for significantly intense reflections: 0.0673
• Weighted residual factors for significantly intense reflections: 0.1716
• Weighted residual factors for all reflections included in the refinement: 0.199
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No