Information card for entry 7133510

Structure parameters

• Formula: C20 H24 Ce38 Cl50 N4 O92
• Calculated formula: C20 H24 Ce38 Cl50 N4 O92
• Title of publication: Isolation of a chloride-capped cerium polyoxo nanocluster built from 52 metal ions.
• Authors of publication: Blanes-Díaz, Anamar; Wacker, Jennifer N.; Szymanowski, Jennifer E. S.; Bertke, Jeffery A.; Knope, Karah E.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 84
• Pages of publication: 12185 - 12188
• a: 18.8106 ± 0.0007 Å
• b: 18.7789 ± 0.0007 Å
• c: 28.4413 ± 0.0011 Å
• α: 90°
• β: 97.602 ± 0.001°
• γ: 90°
• Cell volume: 9958.4 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1104
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1009
• Weighted residual factors for all reflections included in the refinement: 0.1188
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No