Information card for entry 7133592

Structure parameters

• Chemical name: (μ-chloro)-hexakisphenyl-dichloro-di-bismuth tetrakis(3,5-bis(trifluoromethyl)phenyl)borate
• Formula: C68 H42 B Bi2 Cl3 F24
• Calculated formula: C68 H42 B Bi2 Cl3 F24
• Title of publication: Synthesis and characterization of chlorotriarylbismuthonium salts.
• Authors of publication: Kuziola, Jennifer; Nöthling, Nils; Leutzsch, Markus; Cornella, Josep
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 76
• Pages of publication: 10532 - 10535
• a: 12.9043 ± 0.0018 Å
• b: 14.639 ± 0.002 Å
• c: 20.359 ± 0.003 Å
• α: 108.297 ± 0.006°
• β: 98.848 ± 0.007°
• γ: 94.297 ± 0.007°
• Cell volume: 3576.8 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0244
• Residual factor for significantly intense reflections: 0.0217
• Weighted residual factors for significantly intense reflections: 0.0505
• Weighted residual factors for all reflections included in the refinement: 0.0522
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No