Information card for entry 7133697

Structure parameters

• Formula: C52 H73 N O Yb
• Calculated formula: C52 H73 N O Yb
• Title of publication: CO reduction by calcium and ytterbium hydride complexes with a bulky monodentate carbazolyl ligand.
• Authors of publication: Hinz, Alexander; Winkler, Lucas; Sun, Xiaofei
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 80
• Pages of publication: 11291 - 11294
• a: 12.93 ± 0.002 Å
• b: 13.419 ± 0.002 Å
• c: 13.9153 ± 0.0019 Å
• α: 74.266 ± 0.012°
• β: 86.131 ± 0.012°
• γ: 76.624 ± 0.013°
• Cell volume: 2260.9 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1035
• Residual factor for significantly intense reflections: 0.0623
• Weighted residual factors for significantly intense reflections: 0.1334
• Weighted residual factors for all reflections included in the refinement: 0.1695
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No