Information card for entry 7133970

Structure parameters

• Formula: C34 H26 Si
• Calculated formula: C17 H13 Si0.5
• Title of publication: Nickel-catalyzed stereospecific reductive cross-coupling of vinyl chlorosilanes with axially chiral biaryl electrophiles.
• Authors of publication: Yin, Tiantian; Sui, Shiyuan; Li, Shuqi; Chang, Junbiao; Bai, Dachang
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 96
• Pages of publication: 14204 - 14207
• a: 14.5996 ± 0.0002 Å
• b: 9.4264 ± 0.0001 Å
• c: 18.8989 ± 0.0002 Å
• α: 90°
• β: 94.442 ± 0.001°
• γ: 90°
• Cell volume: 2593.09 ± 0.05 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 3
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0631
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for significantly intense reflections: 0.1551
• Weighted residual factors for all reflections included in the refinement: 0.1596
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No