Information card for entry 7134365

Structure parameters

• Formula: C30 H34 N2 O2
• Calculated formula: C30 H34 N2 O2
• Title of publication: Reductive alkylation of azoarenes to N-alkylated hydrazines enabled by hexafluoroisopropanol
• Authors of publication: Senapati, Siddhartha Kumar; Das, Animesh
• Journal of publication: Chemical Communications
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 47
• Pages of publication: 8596 - 8599
• a: 11.5525 ± 0.0008 Å
• b: 7.9187 ± 0.0006 Å
• c: 28.056 ± 0.002 Å
• α: 90°
• β: 96.854 ± 0.002°
• γ: 90°
• Cell volume: 2548.2 ± 0.3 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1246
• Residual factor for significantly intense reflections: 0.0994
• Weighted residual factors for significantly intense reflections: 0.2239
• Weighted residual factors for all reflections included in the refinement: 0.2439
• Goodness-of-fit parameter for all reflections included in the refinement: 1.142
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No