Information card for entry 7134391

Structure parameters

• Formula: C67 H37 B F24 Mo5 O10 P2 Sb2
• Calculated formula: C67 H37 B F24 Mo5 O10 P2 Sb2
• Title of publication: Synthesis of heteropnictogen ligands via PI transfer
• Authors of publication: Zimmermann, Lisa; Land, Michael A.; Riesinger, Christoph; Macdonald, Charles L. B.; Scheer, Manfred
• Journal of publication: Chemical Communications
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 38
• Pages of publication: 6973 - 6976
• a: 18.9232 ± 0.0002 Å
• b: 20.718 ± 0.0002 Å
• c: 20.1171 ± 0.0002 Å
• α: 90°
• β: 113.323 ± 0.001°
• γ: 90°
• Cell volume: 7242.47 ± 0.14 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0508
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.1129
• Weighted residual factors for all reflections included in the refinement: 0.1181
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No