Information card for entry 7134640

Structure parameters

• Formula: C30 H43 Al N2
• Calculated formula: C30 H43 Al N2
• Title of publication: Alkylaluminium-catalyzed regioselective hydrophosphinylation of α,β-unsaturated ketones into γ-ketophosphine oxides
• Authors of publication: Chen, Yiwen; Pang, Ziyuan; Li, Gege; Yang, Xiaobo; Yan, Wenliang; Li, Qifeng; Dong, Xuan; Ma, Xiaoli; Yang, Zhi
• Journal of publication: Chemical Communications
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 53
• Pages of publication: 9666 - 9669
• a: 15.6163 ± 0.0007 Å
• b: 22.5091 ± 0.0009 Å
• c: 7.737 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2719.6 ± 0.2 ų
• Cell temperature: 99.99 ± 0.1 K
• Ambient diffraction temperature: 99.99 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 39
• Hermann-Mauguin space group symbol: A e m 2
• Hall space group symbol: A 2 -2b
• Residual factor for all reflections: 0.067
• Residual factor for significantly intense reflections: 0.0636
• Weighted residual factors for significantly intense reflections: 0.1627
• Weighted residual factors for all reflections included in the refinement: 0.1645
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No