Information card for entry 7134821

Structure parameters

• Formula: C13 H13 Br2 N3 O Zn
• Calculated formula: C13 H13 Br2 N3 O Zn
• Title of publication: Merging metal-ligand cooperation and redox promoted strategy for tailored synthesis of alkylated 9<i>H</i>-fluorenes.
• Authors of publication: Samanta, Arup; Phukan, Hirak Jyoti; Tripathi, Ujjwal Kumar; Srimani, Dipankar
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 67
• Pages of publication: 12582 - 12585
• a: 13.4493 ± 0.001 Å
• b: 15.5797 ± 0.0012 Å
• c: 7.6731 ± 0.0006 Å
• α: 90°
• β: 106.091 ± 0.002°
• γ: 90°
• Cell volume: 1544.8 ± 0.2 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0351
• Residual factor for significantly intense reflections: 0.0318
• Weighted residual factors for significantly intense reflections: 0.1051
• Weighted residual factors for all reflections included in the refinement: 0.1107
• Goodness-of-fit parameter for all reflections included in the refinement: 0.926
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No