Information card for entry 7134824

Structure parameters

• Formula: C19 H18 Cl2
• Calculated formula: C19 H18 Cl2
• Title of publication: Merging metal-ligand cooperation and redox promoted strategy for tailored synthesis of alkylated 9<i>H</i>-fluorenes.
• Authors of publication: Samanta, Arup; Phukan, Hirak Jyoti; Tripathi, Ujjwal Kumar; Srimani, Dipankar
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 67
• Pages of publication: 12582 - 12585
• a: 8.297 ± 0.0008 Å
• b: 9.0505 ± 0.0009 Å
• c: 11.4465 ± 0.0011 Å
• α: 93.075 ± 0.002°
• β: 97.902 ± 0.002°
• γ: 111.839 ± 0.002°
• Cell volume: 785.13 ± 0.13 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0417
• Residual factor for significantly intense reflections: 0.0382
• Weighted residual factors for significantly intense reflections: 0.0955
• Weighted residual factors for all reflections included in the refinement: 0.1001
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No