Crystallography Open Database

Information card for entry 7134843

Preview

Coordinates	7134843.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Co H16 N10 O8
Calculated formula	Co H16 N10 O8
Title of publication	Electrosynthesis of a <i>cyclo</i>-N<sub>5</sub><sup>-</sup> anion <i>via</i> TEMPO-mediated selective C-N bond cleavage in aryl-pentazole.
Authors of publication	Zhao, Feng; Gu, Ziyan; Song, Bin; Ju, Xuehai; Hu, Bingcheng; Zhang, Chong
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2025
Journal volume	61
Journal issue	68
Pages of publication	12725 - 12728
a	6.4648 ± 0.0003 Å
b	12.1663 ± 0.0005 Å
c	17.1617 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	1349.81 ± 0.1 Å³
Cell temperature	193 K
Ambient diffraction temperature	193 K
Number of distinct elements	4
Space group number	69
Hermann-Mauguin space group symbol	F m m m
Hall space group symbol	-F 2 2
Residual factor for all reflections	0.027
Residual factor for significantly intense reflections	0.027
Weighted residual factors for significantly intense reflections	0.0739
Weighted residual factors for all reflections included in the refinement	0.0739
Goodness-of-fit parameter for all reflections included in the refinement	1.173
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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