Information card for entry 7134886

Structure parameters

• Formula: C38 H32 B0.91 F15 Ga1.09
• Calculated formula: C38 H32 B0.9076 F15 Ga1.0924
• Title of publication: 1,2,4-Tri(^<i>t</i>Bu)cyclopentadienyl gallium (Cp'''Ga) as a versatile reagent for the synthesis of Lewis adducts and ionic compounds.
• Authors of publication: Ding, Yi; Tang, Yongheng; Nazish, Mohd; Ruth, Paul Niklas; Wachendorf, Sophia Luisa; Herbst-Irmer, Regine; Stalke, Dietmar; Roesky, Herbert W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 71
• Pages of publication: 13441 - 13444
• a: 10.03 ± 0.002 Å
• b: 12.141 ± 0.002 Å
• c: 15.017 ± 0.003 Å
• α: 77.99 ± 0.02°
• β: 80.13 ± 0.03°
• γ: 78.22 ± 0.02°
• Cell volume: 1735 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0358
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0676
• Weighted residual factors for all reflections included in the refinement: 0.0704
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No