Information card for entry 7134969

Structure parameters

• Formula: C39 H34 Cl3 D O4 Si
• Calculated formula: C39 H34 Cl3 D O4 Si
• Title of publication: Synthesis and characterization of the first neutral hexacoordinated silole complexes.
• Authors of publication: Szathmári, Balázs; Holczbauer, Tamás; Balterer, Bence; Domján, Attila; Volk, Balázs; Kovács, Ilona; Kelemen, Zsolt
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2025
• Journal volume: 61
• Journal issue: 82
• Pages of publication: 16042 - 16045
• a: 11.0558 ± 0.0001 Å
• b: 13.5926 ± 0.0001 Å
• c: 23.5001 ± 0.0001 Å
• α: 90°
• β: 102.655 ± 0.001°
• γ: 90°
• Cell volume: 3445.73 ± 0.04 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 n 1
• Hall space group symbol: P -2yac
• Residual factor for all reflections: 0.0414
• Residual factor for significantly intense reflections: 0.0405
• Weighted residual factors for significantly intense reflections: 0.1107
• Weighted residual factors for all reflections included in the refinement: 0.1117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No