#------------------------------------------------------------------------------
#$Date: 2025-12-04 23:59:04 +0100 (Thu 04 de Dec de 2025) $
#$Revision: 304032 $
#$URL: svn://www.crystallography.net/cod/cif/7/13/52/7135289.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7135289
loop_
_publ_author_name
'Li, Xinrui'
'Zhou, Ningning'
'Tu, Deshuang'
'Lu, Chang-sheng'
'Yan, Hong'
_publ_section_title
;
 Metal-free regioselective B--O coupling in carboranes for constructing
 aggregation-induced emission luminogens
;
_journal_name_full               'Chemical Communications'
_journal_paper_doi               10.1039/D5CC03944D
_journal_year                    2026
_chemical_formula_moiety         'C9 H18 B9 N O2'
_chemical_formula_sum            'C9 H18 B9 N O2'
_chemical_formula_weight         269.53
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_date             2025-08-27
_audit_creation_method
;
Olex2 1.5
(compiled 2025.07.13 svn.rb7424aed for OlexSys, GUI svn.r7314)
;
_audit_update_record
;
2025-09-25 deposited with the CCDC.	2025-11-27 downloaded from the CCDC.
;
_cell_angle_alpha                97.167(14)
_cell_angle_beta                 102.787(13)
_cell_angle_gamma                102.826(14)
_cell_formula_units_Z            2
_cell_length_a                   7.035(3)
_cell_length_b                   9.707(4)
_cell_length_c                   11.990(5)
_cell_measurement_reflns_used    2371
_cell_measurement_temperature    293.0
_cell_measurement_theta_max      27.23
_cell_measurement_theta_min      2.55
_cell_volume                     765.4(6)
_computing_cell_refinement       'SAINT v8.37A (Bruker, 2015)'
_computing_data_collection       'Bruker SMART Apex III CCD diffractometer'
_computing_data_reduction        'SAINT v8.37A (Bruker, 2015)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2014/7 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      293.0
_diffrn_measured_fraction_theta_full 0.987
_diffrn_measured_fraction_theta_max 0.977
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0402
_diffrn_reflns_av_unetI/netI     0.0595
_diffrn_reflns_Laue_measured_fraction_full 0.987
_diffrn_reflns_Laue_measured_fraction_max 0.977
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            6845
_diffrn_reflns_point_group_measured_fraction_full 0.987
_diffrn_reflns_point_group_measured_fraction_max 0.977
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.555
_diffrn_reflns_theta_min         1.772
_diffrn_source_current           40.0
_diffrn_source_power             1.8
_diffrn_source_voltage           45.0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.068
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.5745
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1291 before and 0.0533 after correction.
The Ratio of minimum to maximum transmission is 0.7705.
The λ/2 correction factor is Not present.
;
_exptl_crystal_colour            'clear light colourless'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.169
_exptl_crystal_description       block
_exptl_crystal_F_000             280
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.19
_exptl_crystal_size_min          0.17
_refine_diff_density_max         0.644
_refine_diff_density_min         -0.212
_refine_diff_density_rms         0.042
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.075
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     207
_refine_ls_number_reflns         3461
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.075
_refine_ls_R_factor_all          0.0993
_refine_ls_R_factor_gt           0.0687
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0959P)²+0.2020P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1898
_refine_ls_wR_factor_ref         0.2126
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2303
_reflns_number_total             3461
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d5cc03944d2.cif
_cod_data_source_block           kkkkk_a
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7135289
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.989
_shelx_estimated_absorpt_t_min   0.986
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C006(H006), C008(H008), C009(H009), C00A(H00A), C00C(H00E)
2.b Idealised Me refined as rotating group:
 C00B(H00B,H00C,H00D)
2.c Boron cage BH refined with riding coordinates:
 B00G(H00H), B00H(H00I), B00I(H00J), B00J(H00K), B00K(H00L), B00L(H00M)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O001 O 0.3436(3) 0.41815(19) 0.10581(15) 0.0638(5) Uani 1 1 d . . . . .
N002 N 0.2146(3) 0.24702(19) 0.50226(15) 0.0467(4) Uani 1 1 d . . . . .
O003 O 0.1734(4) 0.5458(2) 0.18960(19) 0.0883(7) Uani 1 1 d . . . . .
C004 C 0.0941(4) 0.1341(3) 0.2725(2) 0.0549(6) Uani 1 1 d . . . . .
C005 C 0.2610(4) 0.5278(3) 0.1165(2) 0.0549(6) Uani 1 1 d . . . . .
C006 C 0.1256(4) 0.3152(3) 0.7111(2) 0.0628(6) Uani 1 1 d . . . . .
H006 H 0.0916 0.3425 0.7936 0.075 Uiso 1 1 calc R U . . .
C007 C 0.1261(4) 0.1808(3) 0.1573(2) 0.0582(6) Uani 1 1 d . . . . .
C008 C 0.0654(4) 0.3124(3) 0.5081(2) 0.0547(6) Uani 1 1 d . . . . .
H008 H -0.0186 0.3379 0.4296 0.066 Uiso 1 1 calc R U . . .
C009 C 0.3181(4) 0.2142(3) 0.5998(2) 0.0576(6) Uani 1 1 d . . . . .
H009 H 0.4361 0.1602 0.5953 0.069 Uiso 1 1 calc R U . . .
C00A C 0.2761(4) 0.2482(3) 0.7048(2) 0.0652(7) Uani 1 1 d . . . . .
H00A H 0.3618 0.2221 0.7825 0.078 Uiso 1 1 calc R U . . .
C00B C 0.2883(4) 0.6225(3) 0.0295(2) 0.0676(7) Uani 1 1 d . . . . .
H00B H 0.4389 0.6373 0.0184 0.101 Uiso 1 1 calc R U . . .
H00C H 0.2650 0.7253 0.0595 0.101 Uiso 1 1 calc R U . . .
H00D H 0.1807 0.5735 -0.0525 0.101 Uiso 1 1 calc R U . . .
C00C C 0.0179(4) 0.3473(3) 0.6113(2) 0.0616(6) Uani 1 1 d . . . . .
H00E H -0.1025 0.3994 0.6142 0.074 Uiso 1 1 calc R U . . .
B00D B 0.2671(4) 0.2170(3) 0.3849(2) 0.0465(6) Uani 1 1 d . . . . .
B00E B 0.4465(4) 0.3462(3) 0.3393(2) 0.0522(6) Uani 1 1 d . . . . .
B00F B 0.3250(4) 0.3139(3) 0.1813(2) 0.0541(6) Uani 1 1 d . . . . .
B00G B 0.4887(4) 0.1778(3) 0.3679(2) 0.0561(7) Uani 1 1 d . . . . .
H00H H 0.6214 0.1764 0.4479 0.067 Uiso 1 1 calc R U . . .
B00H B 0.5311(5) 0.2411(3) 0.2362(2) 0.0595(7) Uani 1 1 d . . . . .
H00I H 0.6929 0.2859 0.2213 0.071 Uiso 1 1 calc R U . . .
B00I B 0.2647(5) 0.0399(3) 0.3286(2) 0.0598(7) Uani 1 1 d . . . . .
H00J H 0.2372 -0.0575 0.3787 0.072 Uiso 1 1 calc R U . . .
B00J B 0.1626(5) 0.0164(3) 0.1771(3) 0.0696(9) Uani 1 1 d . . . . .
H00K H 0.0604 -0.0960 0.1221 0.084 Uiso 1 1 calc R U . . .
B00K B 0.3293(5) 0.1348(3) 0.1215(3) 0.0641(8) Uani 1 1 d . . . . .
H00L H 0.3495 0.1033 0.0269 0.077 Uiso 1 1 calc R U . . .
B00L B 0.4258(6) 0.0528(4) 0.2344(3) 0.0679(8) Uani 1 1 d . . . . .
H00M H 0.5169 -0.0341 0.2201 0.082 Uiso 1 1 calc R U . . .
H00F H 0.295(4) 0.371(3) 0.287(2) 0.066(7) Uiso 1 1 d . . . . .
H00G H 0.547(4) 0.447(3) 0.388(2) 0.061(7) Uiso 1 1 d . . . . .
H007 H 0.005(4) 0.170(3) 0.090(2) 0.078(8) Uiso 1 1 d . . . . .
H004 H -0.045(5) 0.097(3) 0.271(2) 0.075(8) Uiso 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C005 O001 B00F 120.4(2) . . ?
C008 N002 B00D 118.98(18) . . ?
C009 N002 C008 119.3(2) . . ?
C009 N002 B00D 121.7(2) . . ?
C007 C004 B00D 114.4(2) . . ?
C007 C004 B00I 112.0(2) . . ?
C007 C004 B00J 62.37(17) . . ?
C007 C004 H004 113.9(17) . . ?
B00D C004 B00I 63.89(15) . . ?
B00D C004 B00J 115.4(2) . . ?
B00D C004 H004 125.0(17) . . ?
B00I C004 H004 117.8(17) . . ?
B00J C004 B00I 61.12(17) . . ?
B00J C004 H004 109.2(17) . . ?
O001 C005 C00B 113.6(2) . . ?
O003 C005 O001 121.8(2) . . ?
O003 C005 C00B 124.6(2) . . ?
C00A C006 H006 120.3 . . ?
C00A C006 C00C 119.3(2) . . ?
C00C C006 H006 120.3 . . ?
C004 C007 B00F 111.37(19) . . ?
C004 C007 B00J 64.02(17) . . ?
C004 C007 B00K 111.99(19) . . ?
C004 C007 H007 119.6(17) . . ?
B00F C007 B00J 117.5(2) . . ?
B00F C007 B00K 65.43(18) . . ?
B00F C007 H007 121.0(17) . . ?
B00J C007 B00K 61.72(19) . . ?
B00J C007 H007 110.4(17) . . ?
B00K C007 H007 115.5(16) . . ?
N002 C008 H008 119.3 . . ?
N002 C008 C00C 121.5(2) . . ?
C00C C008 H008 119.3 . . ?
N002 C009 H009 119.5 . . ?
N002 C009 C00A 121.0(2) . . ?
C00A C009 H009 119.5 . . ?
C006 C00A C009 119.8(2) . . ?
C006 C00A H00A 120.1 . . ?
C009 C00A H00A 120.1 . . ?
C005 C00B H00B 109.5 . . ?
C005 C00B H00C 109.5 . . ?
C005 C00B H00D 109.5 . . ?
H00B C00B H00C 109.5 . . ?
H00B C00B H00D 109.5 . . ?
H00C C00B H00D 109.5 . . ?
C006 C00C H00E 120.5 . . ?
C008 C00C C006 119.1(2) . . ?
C008 C00C H00E 120.5 . . ?
N002 B00D C004 119.7(2) . . ?
N002 B00D B00E 122.40(19) . . ?
N002 B00D B00G 125.04(19) . . ?
N002 B00D B00I 118.80(19) . . ?
C004 B00D B00E 107.51(19) . . ?
C004 B00D B00G 107.3(2) . . ?
C004 B00D B00I 62.21(16) . . ?
B00G B00D B00E 60.72(16) . . ?
B00G B00D B00I 60.23(17) . . ?
B00I B00D B00E 111.2(2) . . ?
B00D B00E B00F 100.19(18) . . ?
B00D B00E H00F 81.8(13) . . ?
B00D B00E H00G 128.9(13) . . ?
B00F B00E H00F 48.7(12) . . ?
B00F B00E H00G 124.3(13) . . ?
B00G B00E B00D 57.77(15) . . ?
B00G B00E B00F 105.13(18) . . ?
B00G B00E B00H 61.38(16) . . ?
B00G B00E H00F 128.7(13) . . ?
B00G B00E H00G 121.6(13) . . ?
B00H B00E B00D 104.53(19) . . ?
B00H B00E B00F 58.61(15) . . ?
B00H B00E H00F 106.8(12) . . ?
B00H B00E H00G 118.9(13) . . ?
H00F B00E H00G 107.9(18) . . ?
O001 B00F C007 122.5(2) . . ?
O001 B00F B00E 126.1(2) . . ?
O001 B00F B00H 120.8(2) . . ?
O001 B00F B00K 116.0(2) . . ?
O001 B00F H00F 112.1(11) . . ?
C007 B00F B00E 106.31(19) . . ?
C007 B00F B00H 104.6(2) . . ?
C007 B00F B00K 59.68(17) . . ?
C007 B00F H00F 91.7(11) . . ?
B00E B00F H00F 40.4(11) . . ?
B00H B00F B00E 58.94(15) . . ?
B00H B00F B00K 58.76(17) . . ?
B00H B00F H00F 98.9(11) . . ?
B00K B00F B00E 107.18(19) . . ?
B00K B00F H00F 131.8(11) . . ?
B00D B00G B00E 61.51(15) . . ?
B00D B00G H00H 122.6 . . ?
B00D B00G B00H 105.87(18) . . ?
B00D B00G B00I 60.73(16) . . ?
B00D B00G B00L 107.0(2) . . ?
B00E B00G H00H 119.1 . . ?
B00E B00G B00H 59.44(16) . . ?
B00E B00G B00L 109.89(19) . . ?
B00H B00G H00H 123.2 . . ?
B00I B00G B00E 112.29(19) . . ?
B00I B00G H00H 120.1 . . ?
B00I B00G B00H 108.0(2) . . ?
B00I B00G B00L 59.77(18) . . ?
B00L B00G H00H 121.8 . . ?
B00L B00G B00H 60.07(17) . . ?
B00E B00H B00G 59.18(15) . . ?
B00E B00H H00I 119.1 . . ?
B00E B00H B00L 108.7(2) . . ?
B00F B00H B00E 62.45(16) . . ?
B00F B00H B00G 106.37(19) . . ?
B00F B00H H00I 121.4 . . ?
B00F B00H B00L 106.9(2) . . ?
B00G B00H H00I 124.1 . . ?
B00K B00H B00E 112.0(2) . . ?
B00K B00H B00F 61.21(16) . . ?
B00K B00H B00G 105.8(2) . . ?
B00K B00H H00I 121.2 . . ?
B00K B00H B00L 58.33(17) . . ?
B00L B00H B00G 58.92(16) . . ?
B00L B00H H00I 122.9 . . ?
C004 B00I B00D 53.90(14) . . ?
C004 B00I B00G 99.99(18) . . ?
C004 B00I H00J 128.0 . . ?
C004 B00I B00J 59.38(16) . . ?
C004 B00I B00L 102.7(2) . . ?
B00D B00I H00J 124.0 . . ?
B00D B00I B00J 105.52(19) . . ?
B00D B00I B00L 106.7(2) . . ?
B00G B00I B00D 59.03(15) . . ?
B00G B00I H00J 123.0 . . ?
B00G B00I B00J 108.4(2) . . ?
B00G B00I B00L 61.07(18) . . ?
B00J B00I H00J 121.0 . . ?
B00J B00I B00L 59.98(19) . . ?
B00L B00I H00J 122.2 . . ?
C004 B00J B00I 59.50(16) . . ?
C004 B00J H00K 126.7 . . ?
C004 B00J B00K 101.8(2) . . ?
C004 B00J B00L 102.8(2) . . ?
C007 B00J C004 53.60(15) . . ?
C007 B00J B00I 103.6(2) . . ?
C007 B00J H00K 125.8 . . ?
C007 B00J B00K 59.27(17) . . ?
C007 B00J B00L 103.4(2) . . ?
B00I B00J H00K 121.5 . . ?
B00K B00J B00I 108.0(2) . . ?
B00K B00J H00K 122.6 . . ?
B00K B00J B00L 59.27(19) . . ?
B00L B00J B00I 60.02(18) . . ?
B00L B00J H00K 123.8 . . ?
C007 B00K B00F 54.89(15) . . ?
C007 B00K B00H 101.9(2) . . ?
C007 B00K B00J 59.01(18) . . ?
C007 B00K H00L 127.3 . . ?
C007 B00K B00L 104.2(2) . . ?
B00F B00K H00L 122.9 . . ?
B00H B00K B00F 60.03(17) . . ?
B00H B00K H00L 121.7 . . ?
B00J B00K B00F 106.3(2) . . ?
B00J B00K B00H 109.7(2) . . ?
B00J B00K H00L 120.9 . . ?
B00L B00K B00F 109.0(2) . . ?
B00L B00K B00H 62.19(18) . . ?
B00L B00K B00J 60.60(19) . . ?
B00L B00K H00L 120.9 . . ?
B00G B00L B00H 61.01(17) . . ?
B00G B00L H00M 121.9 . . ?
B00H B00L H00M 121.7 . . ?
B00I B00L B00G 59.16(16) . . ?
B00I B00L B00H 108.3(2) . . ?
B00I B00L H00M 121.6 . . ?
B00J B00L B00G 106.9(2) . . ?
B00J B00L B00H 107.2(2) . . ?
B00J B00L B00I 60.00(19) . . ?
B00J B00L H00M 122.4 . . ?
B00K B00L B00G 108.3(2) . . ?
B00K B00L B00H 59.47(18) . . ?
B00K B00L B00I 108.6(2) . . ?
B00K B00L B00J 60.12(19) . . ?
B00K B00L H00M 121.4 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O001 C005 1.327(3) . ?
O001 B00F 1.443(3) . ?
N002 C008 1.352(3) . ?
N002 C009 1.348(3) . ?
N002 B00D 1.542(3) . ?
O003 C005 1.195(3) . ?
C004 C007 1.552(3) . ?
C004 B00D 1.586(3) . ?
C004 B00I 1.736(4) . ?
C004 B00J 1.734(4) . ?
C004 H004 0.96(3) . ?
C005 C00B 1.490(3) . ?
C006 H006 1.0830 . ?
C006 C00A 1.370(4) . ?
C006 C00C 1.378(4) . ?
C007 B00F 1.624(4) . ?
C007 B00J 1.709(4) . ?
C007 B00K 1.713(4) . ?
C007 H007 1.01(3) . ?
C008 H008 1.0830 . ?
C008 C00C 1.373(3) . ?
C009 H009 1.0830 . ?
C009 C00A 1.373(3) . ?
C00A H00A 1.0830 . ?
C00B H00B 1.0770 . ?
C00B H00C 1.0770 . ?
C00B H00D 1.0770 . ?
C00C H00E 1.0830 . ?
B00D B00E 1.800(4) . ?
B00D B00G 1.732(4) . ?
B00D B00I 1.762(4) . ?
B00E B00F 1.853(4) . ?
B00E B00G 1.786(4) . ?
B00E B00H 1.791(4) . ?
B00E H00F 1.20(3) . ?
B00E H00G 1.08(3) . ?
B00F B00H 1.784(4) . ?
B00F B00K 1.805(4) . ?
B00F H00F 1.39(2) . ?
B00G H00H 1.1851 . ?
B00G B00H 1.825(4) . ?
B00G B00I 1.753(4) . ?
B00G B00L 1.787(4) . ?
B00H H00I 1.1851 . ?
B00H B00K 1.761(5) . ?
B00H B00L 1.809(5) . ?
B00I H00J 1.1851 . ?
B00I B00J 1.764(4) . ?
B00I B00L 1.764(5) . ?
B00J H00K 1.1851 . ?
B00J B00K 1.755(5) . ?
B00J B00L 1.764(5) . ?
B00K H00L 1.1851 . ?
B00K B00L 1.740(4) . ?
B00L H00M 1.1851 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O001 B00F B00H B00E 116.2(3) . . . . ?
O001 B00F B00H B00G 157.1(2) . . . . ?
O001 B00F B00H B00K -103.6(3) . . . . ?
O001 B00F B00H B00L -141.1(2) . . . . ?
O001 B00F B00K C007 -114.1(2) . . . . ?
O001 B00F B00K B00H 111.8(3) . . . . ?
O001 B00F B00K B00J -144.5(2) . . . . ?
O001 B00F B00K B00L 151.6(2) . . . . ?
N002 C008 C00C C006 0.2(4) . . . . ?
N002 C009 C00A C006 0.7(4) . . . . ?
N002 B00D B00E B00F -143.4(2) . . . . ?
N002 B00D B00E B00G 115.1(2) . . . . ?
N002 B00D B00E B00H 156.63(19) . . . . ?
N002 B00D B00G B00E -110.9(2) . . . . ?
N002 B00D B00G B00H -151.8(2) . . . . ?
N002 B00D B00G B00I 106.1(2) . . . . ?
N002 B00D B00G B00L 145.3(2) . . . . ?
N002 B00D B00I C004 110.4(2) . . . . ?
N002 B00D B00I B00G -116.1(2) . . . . ?
N002 B00D B00I B00J 141.4(2) . . . . ?
N002 B00D B00I B00L -155.9(2) . . . . ?
C004 C007 B00F O001 -151.5(2) . . . . ?
C004 C007 B00F B00E 4.6(3) . . . . ?
C004 C007 B00F B00H 65.9(2) . . . . ?
C004 C007 B00F B00K 105.3(2) . . . . ?
C004 C007 B00J B00I -34.3(2) . . . . ?
C004 C007 B00J B00K -137.3(2) . . . . ?
C004 C007 B00J B00L -96.2(2) . . . . ?
C004 C007 B00K B00F -104.3(2) . . . . ?
C004 C007 B00K B00H -64.9(3) . . . . ?
C004 C007 B00K B00J 41.1(2) . . . . ?
C004 C007 B00K B00L -0.9(3) . . . . ?
C004 B00D B00E B00F 1.2(2) . . . . ?
C004 B00D B00E B00G -100.4(2) . . . . ?
C004 B00D B00E B00H -58.8(2) . . . . ?
C004 B00D B00G B00E 100.8(2) . . . . ?
C004 B00D B00G B00H 59.9(2) . . . . ?
C004 B00D B00G B00I -42.25(19) . . . . ?
C004 B00D B00G B00L -3.0(3) . . . . ?
C004 B00D B00I B00G 133.5(2) . . . . ?
C004 B00D B00I B00J 31.0(2) . . . . ?
C004 B00D B00I B00L 93.7(2) . . . . ?
C004 B00I B00J C007 31.72(19) . . . . ?
C004 B00I B00J B00K 93.4(2) . . . . ?
C004 B00I B00J B00L 129.6(2) . . . . ?
C004 B00I B00L B00G 94.52(19) . . . . ?
C004 B00I B00L B00H 56.9(2) . . . . ?
C004 B00I B00L B00J -42.85(18) . . . . ?
C004 B00I B00L B00K -6.2(3) . . . . ?
C004 B00J B00K C007 -33.89(17) . . . . ?
C004 B00J B00K B00F -5.0(3) . . . . ?
C004 B00J B00K B00H 58.4(3) . . . . ?
C004 B00J B00K B00L 98.0(2) . . . . ?
C004 B00J B00L B00G 5.5(3) . . . . ?
C004 B00J B00L B00H -58.6(2) . . . . ?
C004 B00J B00L B00I 42.94(18) . . . . ?
C004 B00J B00L B00K -96.3(2) . . . . ?
C005 O001 B00F C007 82.2(3) . . . . ?
C005 O001 B00F B00E -69.0(3) . . . . ?
C005 O001 B00F B00H -141.0(2) . . . . ?
C005 O001 B00F B00K 151.4(2) . . . . ?
C007 C004 B00D N002 147.3(2) . . . . ?
C007 C004 B00D B00E 1.6(3) . . . . ?
C007 C004 B00D B00G -62.4(3) . . . . ?
C007 C004 B00D B00I -103.7(2) . . . . ?
C007 C004 B00I B00D 107.4(2) . . . . ?
C007 C004 B00I B00G 68.2(2) . . . . ?
C007 C004 B00I B00J -37.4(2) . . . . ?
C007 C004 B00I B00L 5.8(3) . . . . ?
C007 C004 B00J B00I 140.6(2) . . . . ?
C007 C004 B00J B00K 36.55(19) . . . . ?
C007 C004 B00J B00L 97.4(2) . . . . ?
C007 B00F B00H B00E -100.5(2) . . . . ?
C007 B00F B00H B00G -59.5(2) . . . . ?
C007 B00F B00H B00K 39.77(19) . . . . ?
C007 B00F B00H B00L 2.2(2) . . . . ?
C007 B00F B00K B00H -134.2(2) . . . . ?
C007 B00F B00K B00J -30.46(19) . . . . ?
C007 B00F B00K B00L -94.4(2) . . . . ?
C007 B00J B00K B00F 28.93(18) . . . . ?
C007 B00J B00K B00H 92.3(2) . . . . ?
C007 B00J B00K B00L 131.9(2) . . . . ?
C007 B00J B00L B00G 60.7(3) . . . . ?
C007 B00J B00L B00H -3.5(3) . . . . ?
C007 B00J B00L B00I 98.1(2) . . . . ?
C007 B00J B00L B00K -41.15(19) . . . . ?
C007 B00K B00L B00G -58.2(3) . . . . ?
C007 B00K B00L B00H -96.2(2) . . . . ?
C007 B00K B00L B00I 4.6(3) . . . . ?
C007 B00K B00L B00J 41.2(2) . . . . ?
C008 N002 C009 C00A -1.0(4) . . . . ?
C008 N002 B00D C004 -52.6(3) . . . . ?
C008 N002 B00D B00E 87.9(3) . . . . ?
C008 N002 B00D B00G 162.7(2) . . . . ?
C008 N002 B00D B00I -125.2(2) . . . . ?
C009 N002 C008 C00C 0.6(3) . . . . ?
C009 N002 B00D C004 129.7(2) . . . . ?
C009 N002 B00D B00E -89.8(3) . . . . ?
C009 N002 B00D B00G -15.0(3) . . . . ?
C009 N002 B00D B00I 57.2(3) . . . . ?
C00A C006 C00C C008 -0.5(4) . . . . ?
C00C C006 C00A C009 0.1(4) . . . . ?
B00D N002 C008 C00C -177.2(2) . . . . ?
B00D N002 C009 C00A 176.7(2) . . . . ?
B00D C004 C007 B00F -4.1(3) . . . . ?
B00D C004 C007 B00J 107.1(2) . . . . ?
B00D C004 C007 B00K 67.0(3) . . . . ?
B00D C004 B00I B00G -39.19(18) . . . . ?
B00D C004 B00I B00J -144.7(2) . . . . ?
B00D C004 B00I B00L -101.6(2) . . . . ?
B00D C004 B00J C007 -105.5(2) . . . . ?
B00D C004 B00J B00I 35.0(2) . . . . ?
B00D C004 B00J B00K -69.0(2) . . . . ?
B00D C004 B00J B00L -8.2(3) . . . . ?
B00D B00E B00F O001 151.6(2) . . . . ?
B00D B00E B00F C007 -3.4(2) . . . . ?
B00D B00E B00F B00H -100.9(2) . . . . ?
B00D B00E B00F B00K -66.0(2) . . . . ?
B00D B00E B00G B00H 133.0(2) . . . . ?
B00D B00E B00G B00I 34.55(19) . . . . ?
B00D B00E B00G B00L 99.1(2) . . . . ?
B00D B00E B00H B00F 93.21(19) . . . . ?
B00D B00E B00H B00G -39.73(17) . . . . ?
B00D B00E B00H B00K 56.0(3) . . . . ?
B00D B00E B00H B00L -6.5(2) . . . . ?
B00D B00G B00H B00E 41.95(18) . . . . ?
B00D B00G B00H B00F -0.6(3) . . . . ?
B00D B00G B00H B00K -64.6(2) . . . . ?
B00D B00G B00H B00L -100.8(2) . . . . ?
B00D B00G B00I C004 36.55(17) . . . . ?
B00D B00G B00I B00J 97.4(2) . . . . ?
B00D B00G B00I B00L 135.61(19) . . . . ?
B00D B00G B00L B00H 98.9(2) . . . . ?
B00D B00G B00L B00I -39.66(18) . . . . ?
B00D B00G B00L B00J -1.8(3) . . . . ?
B00D B00G B00L B00K 61.6(3) . . . . ?
B00D B00I B00J C004 -28.96(19) . . . . ?
B00D B00I B00J C007 2.8(3) . . . . ?
B00D B00I B00J B00K 64.4(3) . . . . ?
B00D B00I B00J B00L 100.6(2) . . . . ?
B00D B00I B00L B00G 38.77(17) . . . . ?
B00D B00I B00L B00H 1.2(3) . . . . ?
B00D B00I B00L B00J -98.6(2) . . . . ?
B00D B00I B00L B00K -61.9(3) . . . . ?
B00E B00D B00G B00H -40.91(18) . . . . ?
B00E B00D B00G B00I -143.0(2) . . . . ?
B00E B00D B00G B00L -103.8(2) . . . . ?
B00E B00D B00I C004 -99.2(2) . . . . ?
B00E B00D B00I B00G 34.25(18) . . . . ?
B00E B00D B00I B00J -68.2(3) . . . . ?
B00E B00D B00I B00L -5.5(3) . . . . ?
B00E B00F B00H B00G 40.93(18) . . . . ?
B00E B00F B00H B00K 140.2(2) . . . . ?
B00E B00F B00H B00L 102.7(2) . . . . ?
B00E B00F B00K C007 99.2(2) . . . . ?
B00E B00F B00K B00H -35.0(2) . . . . ?
B00E B00F B00K B00J 68.7(3) . . . . ?
B00E B00F B00K B00L 4.8(3) . . . . ?
B00E B00G B00H B00F -42.56(19) . . . . ?
B00E B00G B00H B00K -106.5(2) . . . . ?
B00E B00G B00H B00L -142.7(2) . . . . ?
B00E B00G B00I C004 1.7(3) . . . . ?
B00E B00G B00I B00D -34.85(19) . . . . ?
B00E B00G B00I B00J 62.6(3) . . . . ?
B00E B00G B00I B00L 100.8(2) . . . . ?
B00E B00G B00L B00H 33.7(2) . . . . ?
B00E B00G B00L B00I -104.8(2) . . . . ?
B00E B00G B00L B00J -67.0(3) . . . . ?
B00E B00G B00L B00K -3.6(3) . . . . ?
B00E B00H B00K C007 0.9(3) . . . . ?
B00E B00H B00K B00F 37.7(2) . . . . ?
B00E B00H B00K B00J -60.2(3) . . . . ?
B00E B00H B00K B00L -99.1(2) . . . . ?
B00E B00H B00L B00G -33.30(18) . . . . ?
B00E B00H B00L B00I 3.5(3) . . . . ?
B00E B00H B00L B00J 66.8(2) . . . . ?
B00E B00H B00L B00K 104.8(2) . . . . ?
B00F O001 C005 O003 1.6(4) . . . . ?
B00F O001 C005 C00B -178.1(2) . . . . ?
B00F C007 B00J C004 101.7(2) . . . . ?
B00F C007 B00J B00I 67.5(3) . . . . ?
B00F C007 B00J B00K -35.6(2) . . . . ?
B00F C007 B00J B00L 5.5(3) . . . . ?
B00F C007 B00K B00H 39.41(19) . . . . ?
B00F C007 B00K B00J 145.4(2) . . . . ?
B00F C007 B00K B00L 103.4(2) . . . . ?
B00F B00E B00G B00D -92.65(19) . . . . ?
B00F B00E B00G B00H 40.34(18) . . . . ?
B00F B00E B00G B00I -58.1(2) . . . . ?
B00F B00E B00G B00L 6.4(3) . . . . ?
B00F B00E B00H B00G -132.9(2) . . . . ?
B00F B00E B00H B00K -37.2(2) . . . . ?
B00F B00E B00H B00L -99.7(2) . . . . ?
B00F B00H B00K C007 -36.83(17) . . . . ?
B00F B00H B00K B00J -97.9(2) . . . . ?
B00F B00H B00K B00L -136.8(2) . . . . ?
B00F B00H B00L B00G -99.3(2) . . . . ?
B00F B00H B00L B00I -62.4(2) . . . . ?
B00F B00H B00L B00J 0.9(3) . . . . ?
B00F B00H B00L B00K 38.8(2) . . . . ?
B00F B00K B00L B00G -0.9(3) . . . . ?
B00F B00K B00L B00H -38.9(2) . . . . ?
B00F B00K B00L B00I 61.9(3) . . . . ?
B00F B00K B00L B00J 98.5(2) . . . . ?
B00G B00D B00E B00F 101.55(19) . . . . ?
B00G B00D B00E B00H 41.55(18) . . . . ?
B00G B00D B00I C004 -133.5(2) . . . . ?
B00G B00D B00I B00J -102.4(2) . . . . ?
B00G B00D B00I B00L -39.73(19) . . . . ?
B00G B00E B00F O001 -149.2(2) . . . . ?
B00G B00E B00F C007 55.8(2) . . . . ?
B00G B00E B00F B00H -41.73(19) . . . . ?
B00G B00E B00F B00K -6.8(3) . . . . ?
B00G B00E B00H B00F 132.9(2) . . . . ?
B00G B00E B00H B00K 95.7(2) . . . . ?
B00G B00E B00H B00L 33.20(19) . . . . ?
B00G B00H B00K C007 63.5(2) . . . . ?
B00G B00H B00K B00F 100.3(2) . . . . ?
B00G B00H B00K B00J 2.4(3) . . . . ?
B00G B00H B00K B00L -36.46(19) . . . . ?
B00G B00H B00L B00I 36.81(19) . . . . ?
B00G B00H B00L B00J 100.1(2) . . . . ?
B00G B00H B00L B00K 138.1(2) . . . . ?
B00G B00I B00J C004 -90.9(2) . . . . ?
B00G B00I B00J C007 -59.2(3) . . . . ?
B00G B00I B00J B00K 2.5(3) . . . . ?
B00G B00I B00J B00L 38.7(2) . . . . ?
B00G B00I B00L B00H -37.62(19) . . . . ?
B00G B00I B00L B00J -137.4(2) . . . . ?
B00G B00I B00L B00K -100.7(2) . . . . ?
B00H B00E B00F O001 -107.5(3) . . . . ?
B00H B00E B00F C007 97.5(2) . . . . ?
B00H B00E B00F B00K 34.9(2) . . . . ?
B00H B00E B00G B00D -133.0(2) . . . . ?
B00H B00E B00G B00I -98.4(2) . . . . ?
B00H B00E B00G B00L -33.9(2) . . . . ?
B00H B00F B00K C007 134.2(2) . . . . ?
B00H B00F B00K B00J 103.7(2) . . . . ?
B00H B00F B00K B00L 39.8(2) . . . . ?
B00H B00G B00I C004 -61.9(2) . . . . ?
B00H B00G B00I B00D -98.5(2) . . . . ?
B00H B00G B00I B00J -1.0(3) . . . . ?
B00H B00G B00I B00L 37.14(19) . . . . ?
B00H B00G B00L B00I -138.5(2) . . . . ?
B00H B00G B00L B00J -100.7(2) . . . . ?
B00H B00G B00L B00K -37.3(2) . . . . ?
B00H B00K B00L B00G 38.0(2) . . . . ?
B00H B00K B00L B00I 100.7(2) . . . . ?
B00H B00K B00L B00J 137.3(2) . . . . ?
B00I C004 C007 B00F -74.4(2) . . . . ?
B00I C004 C007 B00J 36.9(2) . . . . ?
B00I C004 C007 B00K -3.2(3) . . . . ?
B00I C004 B00D N002 -109.1(2) . . . . ?
B00I C004 B00D B00E 105.2(2) . . . . ?
B00I C004 B00D B00G 41.28(19) . . . . ?
B00I C004 B00J C007 -140.6(2) . . . . ?
B00I C004 B00J B00K -104.0(2) . . . . ?
B00I C004 B00J B00L -43.22(19) . . . . ?
B00I B00D B00E B00F 67.5(2) . . . . ?
B00I B00D B00E B00G -34.07(18) . . . . ?
B00I B00D B00E B00H 7.5(2) . . . . ?
B00I B00D B00G B00E 143.0(2) . . . . ?
B00I B00D B00G B00H 102.1(2) . . . . ?
B00I B00D B00G B00L 39.20(19) . . . . ?
B00I B00G B00H B00E 105.7(2) . . . . ?
B00I B00G B00H B00F 63.2(2) . . . . ?
B00I B00G B00H B00K -0.8(3) . . . . ?
B00I B00G B00H B00L -37.0(2) . . . . ?
B00I B00G B00L B00H 138.5(2) . . . . ?
B00I B00G B00L B00J 37.8(2) . . . . ?
B00I B00G B00L B00K 101.2(3) . . . . ?
B00I B00J B00K C007 -95.4(2) . . . . ?
B00I B00J B00K B00F -66.5(3) . . . . ?
B00I B00J B00K B00H -3.1(3) . . . . ?
B00I B00J B00K B00L 36.5(2) . . . . ?
B00I B00J B00L B00G -37.43(19) . . . . ?
B00I B00J B00L B00H -101.6(2) . . . . ?
B00I B00J B00L B00K -139.2(2) . . . . ?
B00J C004 C007 B00F -111.2(2) . . . . ?
B00J C004 C007 B00K -40.1(2) . . . . ?
B00J C004 B00D N002 -143.1(2) . . . . ?
B00J C004 B00D B00E 71.2(2) . . . . ?
B00J C004 B00D B00G 7.2(3) . . . . ?
B00J C004 B00D B00I -34.0(2) . . . . ?
B00J C004 B00I B00D 144.7(2) . . . . ?
B00J C004 B00I B00G 105.5(2) . . . . ?
B00J C004 B00I B00L 43.2(2) . . . . ?
B00J C007 B00F O001 137.6(2) . . . . ?
B00J C007 B00F B00E -66.4(3) . . . . ?
B00J C007 B00F B00H -5.0(3) . . . . ?
B00J C007 B00F B00K 34.3(2) . . . . ?
B00J C007 B00K B00F -145.4(2) . . . . ?
B00J C007 B00K B00H -106.0(2) . . . . ?
B00J C007 B00K B00L -42.0(2) . . . . ?
B00J B00I B00L B00G 137.4(2) . . . . ?
B00J B00I B00L B00H 99.7(2) . . . . ?
B00J B00I B00L B00K 36.7(2) . . . . ?
B00J B00K B00L B00G -99.4(2) . . . . ?
B00J B00K B00L B00H -137.3(2) . . . . ?
B00J B00K B00L B00I -36.6(2) . . . . ?
B00K C007 B00F O001 103.3(3) . . . . ?
B00K C007 B00F B00E -100.7(2) . . . . ?
B00K C007 B00F B00H -39.32(18) . . . . ?
B00K C007 B00J C004 137.3(2) . . . . ?
B00K C007 B00J B00I 103.1(2) . . . . ?
B00K C007 B00J B00L 41.1(2) . . . . ?
B00K B00F B00H B00E -140.2(2) . . . . ?
B00K B00F B00H B00G -99.3(2) . . . . ?
B00K B00F B00H B00L -37.5(2) . . . . ?
B00K B00H B00L B00G -138.1(2) . . . . ?
B00K B00H B00L B00I -101.3(2) . . . . ?
B00K B00H B00L B00J -38.0(2) . . . . ?
B00K B00J B00L B00G 101.8(2) . . . . ?
B00K B00J B00L B00H 37.7(2) . . . . ?
B00K B00J B00L B00I 139.2(2) . . . . ?
B00L B00G B00H B00E 142.7(2) . . . . ?
B00L B00G B00H B00F 100.2(2) . . . . ?
B00L B00G B00H B00K 36.2(2) . . . . ?
B00L B00G B00I C004 -99.1(2) . . . . ?
B00L B00G B00I B00D -135.61(19) . . . . ?
B00L B00G B00I B00J -38.2(2) . . . . ?
B00L B00H B00K C007 99.9(2) . . . . ?
B00L B00H B00K B00F 136.8(2) . . . . ?
B00L B00H B00K B00J 38.8(2) . . . . ?
B00L B00I B00J C004 -129.6(2) . . . . ?
B00L B00I B00J C007 -97.8(2) . . . . ?
B00L B00I B00J B00K -36.2(2) . . . . ?
B00L B00J B00K C007 -131.9(2) . . . . ?
B00L B00J B00K B00F -102.9(2) . . . . ?
B00L B00J B00K B00H -39.6(2) . . . . ?
