Crystallography Open Database

Information card for entry 7135547

Preview

Coordinates	7135547.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C78 H210 Cu Ge18 K O6 Si24
Calculated formula	C78 H210 Cu Ge18 K O6 Si24
Title of publication	Stepwise coordination of {Cu(C<sub>5</sub>Me<sub>5</sub>)} with a tri-silylated Ge<sub>9</sub> cluster.
Authors of publication	Chen, Tianzi; Wang, Xinyue; Han, Yulin; Guo, Chenxi; Duan, Dongyu; Tang, Yu; Pan, Fuxing
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2026
Journal volume	62
Journal issue	11
Pages of publication	3541 - 3544
a	23.6847 ± 0.0004 Å
b	23.6847 ± 0.0004 Å
c	23.4153 ± 0.0006 Å
α	90°
β	90°
γ	120°
Cell volume	11375.4 ± 0.4 Å³
Cell temperature	150.15 K
Ambient diffraction temperature	150.15 K
Number of distinct elements	7
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.0494
Residual factor for significantly intense reflections	0.0399
Weighted residual factors for significantly intense reflections	0.0912
Weighted residual factors for all reflections included in the refinement	0.0952
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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