Information card for entry 7135631

Structure parameters

• Formula: C89 H134.5 K O7.25 Pb2
• Calculated formula: C84 H122 K O6 Pb2
• Title of publication: Large shortening of the lead-lead bond in a diplumbyne upon its one-electron reduction
• Authors of publication: Queen, Joshua D.; Power, Philip P.
• Journal of publication: Chemical Communications
• Year of publication: 2026
• a: 15.9819 ± 0.0004 Å
• b: 16.1583 ± 0.0003 Å
• c: 22.8325 ± 0.0005 Å
• α: 75.341 ± 0.001°
• β: 70.595 ± 0.001°
• γ: 65.844 ± 0.001°
• Cell volume: 5027.2 ± 0.2 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0713
• Residual factor for significantly intense reflections: 0.0654
• Weighted residual factors for significantly intense reflections: 0.1985
• Weighted residual factors for all reflections included in the refinement: 0.2089
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No