Information card for entry 7150404

Structure parameters

• Common name: RWX0315/Wilson/NW-G020/5107/25-9-98.
• Formula: C38 H51 N3 O2
• Calculated formula: C37.5 H47 N2.5 O2
• Title of publication: Diastereoselective synthesis of atropisomers containing two non-biaryl stereogenic axes: stereochemical relay through stereogenic centres in dihydrostilbene-2,2'-dicarboxamides.
• Authors of publication: Clayden, Jonathan; Westlund, Neil; Frampton, Christopher S.; Helliwell, Madeleine
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2006
• Journal volume: 4
• Journal issue: 3
• Pages of publication: 455 - 461
• a: 15.179 ± 0.003 Å
• b: 7.728 ± 0.002 Å
• c: 28.337 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3324 ± 1.3 ų
• Cell temperature: 123 ± 1 K
• Ambient diffraction temperature: 123 ± 1 K
• Number of distinct elements: 4
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.1178
• Weighted residual factors for all reflections included in the refinement: 0.1249
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No