Information card for entry 7150518

Structure parameters

• Formula: C13 H24 Cl3 N3 O5 Os
• Calculated formula: C13 H24 Cl3 N3 O5 Os
• SMILES: [Os]12(O[C@H]3CC(NC(=O)C(Cl)(Cl)Cl)C[C@H]3O1)(=O)(=O)[N](CC[N]2(C)C)(C)C
• Title of publication: Scope of the directed dihydroxylation: application to cyclic homoallylic alcohols and trihaloacetamides
• Authors of publication: Donohoe, Timothy J.; Mitchell, Lee; Waring, Michael J.; Helliwell, Madeleine; Bell, Andrew; Newcombe, Nicholas J.
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2003
• Journal volume: 1
• Journal issue: 12
• Pages of publication: 2173
• a: 11.19 ± 0.02 Å
• b: 11.405 ± 0.01 Å
• c: 15.857 ± 0.01 Å
• α: 90°
• β: 102.57 ± 0.04°
• γ: 90°
• Cell volume: 1975 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0261
• Residual factor for significantly intense reflections: 0.024
• Weighted residual factors for significantly intense reflections: 0.0619
• Weighted residual factors for all reflections included in the refinement: 0.0629
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No