Information card for entry 7151251
| Formula |
C25 H26 N2 O2 |
| Calculated formula |
C25 H26 N2 O2 |
| SMILES |
C1CCC2c3c1c(C(=O)OC)c(c1ccccc1)n3CCN2Cc1ccccc1 |
| Title of publication |
Intramolecular 1,3-dipolar cycloadditions of dihydroimidazolium ylides: synthesis of pyrrolo[1,2,3-de]quinoxalines and imidazo[1,2-a]indoles. |
| Authors of publication |
Lory, Pedro M. J.; Jones, Raymond C. F.; Iley, James N.; Coles, Simon J.; Hursthouse, Michael B. |
| Journal of publication |
Organic & biomolecular chemistry |
| Year of publication |
2006 |
| Journal volume |
4 |
| Journal issue |
16 |
| Pages of publication |
3155 - 3165 |
| a |
11.448 ± 0.002 Å |
| b |
11.905 ± 0.002 Å |
| c |
15.067 ± 0.003 Å |
| α |
86.5 ± 0.03° |
| β |
87.96 ± 0.03° |
| γ |
77.45 ± 0.03° |
| Cell volume |
2000.1 ± 0.7 Å3 |
| Cell temperature |
150 ± 2 K |
| Ambient diffraction temperature |
150 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.2781 |
| Residual factor for significantly intense reflections |
0.0682 |
| Weighted residual factors for significantly intense reflections |
0.1036 |
| Weighted residual factors for all reflections included in the refinement |
0.1613 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.867 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7151251.html
