Pyrrolyl-, 2-(2-thienyl)pyrrolyl- and 2,5-bis(2-thienyl)pyrrolyl-nucleosides: synthesis, molecular and electronic structure, and redox behaviour of C5-thymidine derivatives.
Authors of publication
Galindo, Miguel A.; Hannant, Jennifer; Harrington, Ross W.; Clegg, William; Horrocks, Benjamin R.; Pike, Andrew R.; Houlton, Andrew
Journal of publication
Organic & biomolecular chemistry
Year of publication
2011
Journal volume
9
Journal issue
5
Pages of publication
1555 - 1564
a
18.3919 ± 0.0005 Å
b
16.7137 ± 0.0005 Å
c
9.28 ± 0.0003 Å
α
90°
β
103.914 ± 0.003°
γ
90°
Cell volume
2768.94 ± 0.15 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0535
Residual factor for significantly intense reflections
0.0389
Weighted residual factors for significantly intense reflections
0.1038
Weighted residual factors for all reflections included in the refinement
0.1103
Goodness-of-fit parameter for all reflections included in the refinement
