Pyrrolyl-, 2-(2-thienyl)pyrrolyl- and 2,5-bis(2-thienyl)pyrrolyl-nucleosides: synthesis, molecular and electronic structure, and redox behaviour of C5-thymidine derivatives.
Authors of publication
Galindo, Miguel A.; Hannant, Jennifer; Harrington, Ross W.; Clegg, William; Horrocks, Benjamin R.; Pike, Andrew R.; Houlton, Andrew
Journal of publication
Organic & biomolecular chemistry
Year of publication
2011
Journal volume
9
Journal issue
5
Pages of publication
1555 - 1564
a
8.0959 ± 0.0004 Å
b
5.7246 ± 0.0003 Å
c
22.417 ± 0.0009 Å
α
90°
β
95.369 ± 0.004°
γ
90°
Cell volume
1034.38 ± 0.09 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0903
Residual factor for significantly intense reflections
0.0578
Weighted residual factors for significantly intense reflections
0.1278
Weighted residual factors for all reflections included in the refinement
0.1445
Goodness-of-fit parameter for all reflections included in the refinement
