Information card for entry 7151985

Structure parameters

• Formula: C159 H215 N8 O50.5 Rh4
• Calculated formula: C158 H170 N8 O50.5 Rh4
• Title of publication: Optimizing dirhodium(ii) tetrakiscarboxylates as chiral NMR auxiliaries.
• Authors of publication: Mattiza, Jens T.; Fohrer, Joerg G. G.; Duddeck, Helmut; Gardiner, Michael G.; Ghanem, Ashraf
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2011
• Journal volume: 9
• Journal issue: 19
• Pages of publication: 6542 - 6550
• a: 28.965 ± 0.014 Å
• b: 36.811 ± 0.018 Å
• c: 15.395 ± 0.016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 16415 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0488
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.1014
• Weighted residual factors for all reflections included in the refinement: 0.1054
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.710673 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No