Helicity discrimination in N,N'-dibenzoyl-1,2,3,4,7,8,9,10-octahydro-1,10-phenanthrolines and their thiono- and selenocarbonyl analogues by inclusion complexation with chiral diols.
Authors of publication
Olszewska, Teresa; Sikorski, Artur; Herman, Aleksander; Połoński, Tadeusz
Journal of publication
Organic & biomolecular chemistry
Year of publication
2013
Journal volume
11
Journal issue
43
Pages of publication
7522 - 7529
a
9.598 ± 0.002 Å
b
16.561 ± 0.003 Å
c
13.354 ± 0.003 Å
α
90°
β
98.05 ± 0.03°
γ
90°
Cell volume
2101.7 ± 0.8 Å3
Cell temperature
295 ± 2 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.1979
Residual factor for significantly intense reflections
0.062
Weighted residual factors for significantly intense reflections
0.1158
Weighted residual factors for all reflections included in the refinement
0.1581
Goodness-of-fit parameter for all reflections included in the refinement
