Helicity discrimination in N,N'-dibenzoyl-1,2,3,4,7,8,9,10-octahydro-1,10-phenanthrolines and their thiono- and selenocarbonyl analogues by inclusion complexation with chiral diols.
Authors of publication
Olszewska, Teresa; Sikorski, Artur; Herman, Aleksander; Połoński, Tadeusz
Journal of publication
Organic & biomolecular chemistry
Year of publication
2013
Journal volume
11
Journal issue
43
Pages of publication
7522 - 7529
a
16.387 ± 0.003 Å
b
9.477 ± 0.002 Å
c
23.828 ± 0.005 Å
α
90°
β
103.58 ± 0.03°
γ
90°
Cell volume
3597 ± 1.3 Å3
Cell temperature
295 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
5
Space group number
5
Hermann-Mauguin space group symbol
C 1 2 1
Hall space group symbol
C 2y
Residual factor for all reflections
0.1038
Residual factor for significantly intense reflections
0.0974
Weighted residual factors for significantly intense reflections
0.2276
Weighted residual factors for all reflections included in the refinement
0.2313
Goodness-of-fit parameter for all reflections included in the refinement
