Information card for entry 7153650

Structure parameters

• Common name: gamma-lactam
• Formula: C40 H28 Cl7 N2 O7 P S
• Calculated formula: C40 H28 Cl7 N2 O7 P S
• Title of publication: One-pot formation of fluorescent γ-lactams having an α-phosphorus ylide moiety through three-component α(δ')-Michael reactions of phosphines with an enyne and N-tosyl aldimines.
• Authors of publication: Lin, Yu-Wei; Deng, Jie-Cheng; Hsieh, You-Zung; Chuang, Shih-Ching
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2014
• Journal volume: 12
• Journal issue: 1
• Pages of publication: 162 - 170
• a: 10.2628 ± 0.0016 Å
• b: 14.104 ± 0.002 Å
• c: 15.146 ± 0.002 Å
• α: 85.999 ± 0.003°
• β: 73.595 ± 0.003°
• γ: 79.998 ± 0.003°
• Cell volume: 2070.6 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1074
• Residual factor for significantly intense reflections: 0.0726
• Weighted residual factors for significantly intense reflections: 0.1825
• Weighted residual factors for all reflections included in the refinement: 0.2043
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No