Information card for entry 7154179

Structure parameters

• Formula: C16 H24 F2 N2 O2 S
• Calculated formula: C16 H24 F2 N2 O2 S
• Title of publication: L-Valine derived chiral N-sulfinamides as effective organocatalysts for the asymmetric hydrosilylation of N-alkyl and N-aryl protected ketimines.
• Authors of publication: Wang, Chao; Wu, Xinjun; Zhou, Li; Sun, Jian
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2015
• Journal volume: 13
• Journal issue: 2
• Pages of publication: 577 - 582
• a: 9.3912 ± 0.0005 Å
• b: 10.6576 ± 0.0004 Å
• c: 18.9928 ± 0.0008 Å
• α: 90°
• β: 94.82 ± 0.002°
• γ: 90°
• Cell volume: 1894.22 ± 0.15 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0326
• Residual factor for significantly intense reflections: 0.0304
• Weighted residual factors for significantly intense reflections: 0.0832
• Weighted residual factors for all reflections included in the refinement: 0.0854
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No