Information card for entry 7154620

Structure parameters

• Formula: C27 H50 N2 O3 Si5
• Calculated formula: C27 H50 N2 O3 Si5
• SMILES: [Si]12(N=NC(=C(O1)c1ccccc1)C(=O)OCC)C([Si](C)(C)C)([Si](C)(C)C)CCC2([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Elusive 2H-1,2-oxasiletes through reactions of an isolable dialkylsilylene with diazocarbonyl compounds.
• Authors of publication: Dong, Zhaowen; Xiao, Xu-Qiong; Li, Zhifang; Lu, Qiong; Lai, Guoqiao; Kira, Mitsuo
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2015
• Journal volume: 13
• Journal issue: 36
• Pages of publication: 9471 - 9476
• a: 9.7059 ± 0.0011 Å
• b: 12.3889 ± 0.0014 Å
• c: 14.2286 ± 0.0016 Å
• α: 93.485 ± 0.002°
• β: 91.21 ± 0.002°
• γ: 97.443 ± 0.002°
• Cell volume: 1692.6 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.059
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.126
• Weighted residual factors for all reflections included in the refinement: 0.1423
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No