I2-TBHP-catalyzed one-pot highly efficient synthesis of 4,3-fused 1,2,4-triazoles from N-tosylhydrazones and aromatic N-heterocycles via intermolecular formal 1,3-dipolar cycloaddition.
Authors of publication
Inturi, Surendra Babu; Kalita, Biswajit; Ahamed, A. Jafar
Journal of publication
Organic & biomolecular chemistry
Year of publication
2016
Journal volume
14
Journal issue
47
Pages of publication
11061 - 11064
a
7.5325 ± 0.0007 Å
b
8.2606 ± 0.0007 Å
c
9.0301 ± 0.0008 Å
α
73.705 ± 0.008°
β
83.998 ± 0.008°
γ
68.21 ± 0.008°
Cell volume
500.78 ± 0.08 Å3
Cell temperature
295 ± 2 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
3
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0625
Residual factor for significantly intense reflections
0.0493
Weighted residual factors for significantly intense reflections
0.098
Weighted residual factors for all reflections included in the refinement
0.1054
Goodness-of-fit parameter for all reflections included in the refinement
