Information card for entry 7155711

Structure parameters

• Formula: C19 H13 F17 N2 O
• Calculated formula: C19 H13 F17 N2 O
• Title of publication: Visible-light mediated directed perfluoroalkylation of hydrazones
• Authors of publication: Ji, Heng; Ni, Hui-qiong; Zhi, Peng; Xi, Zi-wei; Wang, Wei; Shi, Jian-jun; Shen, Yong-miao
• Journal of publication: Org. Biomol. Chem.
• Year of publication: 2017
• a: 21.57 ± 0.004 Å
• b: 5.4827 ± 0.0009 Å
• c: 19.132 ± 0.003 Å
• α: 90°
• β: 104.557 ± 0.004°
• γ: 90°
• Cell volume: 2190 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1492
• Residual factor for significantly intense reflections: 0.1024
• Weighted residual factors for significantly intense reflections: 0.263
• Weighted residual factors for all reflections included in the refinement: 0.2893
• Goodness-of-fit parameter for all reflections included in the refinement: 1.161
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No