Information card for entry 7156145

Structure parameters

• Formula: C33 H25 O2 P
• Calculated formula: C33 H25 O2 P
• Title of publication: Eosin Y-catalyzed, visible-light-promoted carbophosphinylation of allylic alcohols via a radical neophyl rearrangement.
• Authors of publication: Yin, Yao; Weng, Wei-Zhi; Sun, Jian-Guo; Zhang, Bo
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2018
• Journal volume: 16
• Journal issue: 13
• Pages of publication: 2356 - 2361
• a: 11.149 ± 0.002 Å
• b: 11.921 ± 0.002 Å
• c: 18.456 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2452.9 ± 0.8 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0505
• Residual factor for significantly intense reflections: 0.0459
• Weighted residual factors for significantly intense reflections: 0.1252
• Weighted residual factors for all reflections included in the refinement: 0.1304
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No