Crystallography Open Database

Information card for entry 7156268

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Structure parameters

Formula	C24 H32 Br O4 P
Calculated formula	C24 H32 Br O4 P
Title of publication	Base-mediated 1,6-conjugate addition of the Seyferth-Gilbert reagent to para-quinone methides.
Authors of publication	Gupta, Ashis Kumar; Ahamad, Shakir; Vaishanv, Narendra Kumar; Kant, Ruchir; Mohanan, Kishor
Journal of publication	Organic & biomolecular chemistry
Year of publication	2018
Journal volume	16
Journal issue	25
Pages of publication	4623 - 4627
a	10.215 ± 0.0009 Å
b	11.4694 ± 0.0012 Å
c	12.0747 ± 0.0013 Å
α	115.285 ± 0.01°
β	93.898 ± 0.008°
γ	92.846 ± 0.008°
Cell volume	1271.3 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2108
Residual factor for significantly intense reflections	0.0793
Weighted residual factors for significantly intense reflections	0.193
Weighted residual factors for all reflections included in the refinement	0.2998
Goodness-of-fit parameter for all reflections included in the refinement	0.979
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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