Information card for entry 7156693
| Formula |
C24 H27 N O3 S |
| Calculated formula |
C24 H27 N O3 S |
| Title of publication |
Palladium-catalyzed intermolecular [4 + 2] formal cycloaddition with (Z)-3-iodo allylic nucleophiles and allenamides. |
| Authors of publication |
Yan, Fachao; Liang, Hanbing; Ai, Bing; Liang, Wenjing; Jiao, Luyang; Yao, Shuzhi; Zhao, Pingping; Liu, Qing; Dong, Yunhui; Liu, Hui |
| Journal of publication |
Organic & biomolecular chemistry |
| Year of publication |
2019 |
| Journal volume |
17 |
| Journal issue |
10 |
| Pages of publication |
2651 - 2656 |
| a |
8.9412 ± 0.0015 Å |
| b |
11.6147 ± 0.0019 Å |
| c |
11.727 ± 0.002 Å |
| α |
92.06 ± 0.005° |
| β |
111.91 ± 0.005° |
| γ |
102.119 ± 0.005° |
| Cell volume |
1095.9 ± 0.3 Å3 |
| Cell temperature |
296 ± 2 K |
| Ambient diffraction temperature |
296 ± 2 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0904 |
| Residual factor for significantly intense reflections |
0.0453 |
| Weighted residual factors for significantly intense reflections |
0.1017 |
| Weighted residual factors for all reflections included in the refinement |
0.12 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.003 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7156693.html
