Information card for entry 7157116

Structure parameters

• Formula: C24 H23 Cl N2 O4 S2
• Calculated formula: C24 H23 Cl N2 O4 S2
• Title of publication: Iodine-mediated aminosulfonylation of alkenyl sulfonamides with sulfonyl hydrazides: synthesis of sulfonylmethyl piperidines, pyrrolidines and pyrazolines.
• Authors of publication: Xu, Zhong-Qi; Wang, Wen-Bo; Zheng, Lin-Chuang; Li, Lin; Duan, Lili; Li, Yue-Ming
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2019
• Journal volume: 17
• Journal issue: 40
• Pages of publication: 9026 - 9038
• a: 10.622 ± 0.002 Å
• b: 10.722 ± 0.002 Å
• c: 11.698 ± 0.002 Å
• α: 78.63 ± 0.03°
• β: 78.84 ± 0.03°
• γ: 67.46 ± 0.03°
• Cell volume: 1196.1 ± 0.5 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.057
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.1104
• Weighted residual factors for all reflections included in the refinement: 0.119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No