Information card for entry 7159929

Structure parameters

• Formula: C24 H25 N O4
• Calculated formula: C24 H25 N O4
• Title of publication: Highly enantio- and diastereoselective construction of spirocyclic oxindoles <i>via</i> a palladium-catalyzed decarboxylative asymmetric [4 + 2] annulation strategy.
• Authors of publication: You, Pengyuan; Liu, Minjie; Zhang, Ke; Yang, Fan; Tan, Zequn; Chen, Fener
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2024
• Journal volume: 22
• Journal issue: 22
• Pages of publication: 4466 - 4471
• a: 8.0358 ± 0.0003 Å
• b: 10.9125 ± 0.0004 Å
• c: 12.2549 ± 0.0005 Å
• α: 90°
• β: 90.715 ± 0.001°
• γ: 90°
• Cell volume: 1074.56 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0305
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.078
• Weighted residual factors for all reflections included in the refinement: 0.0793
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No