Information card for entry 7160089

Structure parameters

• Common name: 2a
• Chemical name: tricycloalkane
• Formula: C64 H132 Si4
• Calculated formula: C64 H132 Si4
• Title of publication: Ring-closing metathesis of dialkenylcycloalkanes for the synthesis of fused bicycloalkanes and tricycloalkanes.
• Authors of publication: Tu, Yuyang; Inagaki, Yusuke; Ohara, Kazuaki; Yamaguchi, Kentaro; Setaka, Wataru
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2024
• Journal volume: 22
• Journal issue: 34
• Pages of publication: 6950 - 6954
• a: 10.0201 ± 0.001 Å
• b: 13.7449 ± 0.0013 Å
• c: 13.8357 ± 0.0013 Å
• α: 114.915 ± 0.006°
• β: 92.11 ± 0.005°
• γ: 92.923 ± 0.005°
• Cell volume: 1722.4 ± 0.3 ų
• Cell temperature: 250 ± 2 K
• Ambient diffraction temperature: 250 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1002
• Residual factor for significantly intense reflections: 0.0731
• Weighted residual factors for significantly intense reflections: 0.1837
• Weighted residual factors for all reflections included in the refinement: 0.2109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No