Information card for entry 7160520

Structure parameters

• Formula: C18 H13 F4 N O2
• Calculated formula: C18 H13 F4 N O2
• Title of publication: Silver-catalyzed generation of acyl radicals from α-imino-oxy acids: access to acylated 3-CF₃-2-oxindoles.
• Authors of publication: Cao, Yating; Wei, Yushan; Hu, Yingxin; Liu, Daosheng; Liu, Mengyao; Wang, Jingjing; Li, Chong; Wang, Pinpin; Hu, Liyan; Li, Feng
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2025
• Journal volume: 23
• Journal issue: 21
• Pages of publication: 5106 - 5110
• a: 8.8404 ± 0.0002 Å
• b: 11.5522 ± 0.0003 Å
• c: 15.9026 ± 0.0004 Å
• α: 90°
• β: 98.593 ± 0.001°
• γ: 90°
• Cell volume: 1605.84 ± 0.07 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.0576
• Weighted residual factors for significantly intense reflections: 0.1432
• Weighted residual factors for all reflections included in the refinement: 0.1638
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No