Information card for entry 7160539

Structure parameters

• Formula: C32 H33 N3 O6
• Calculated formula: C32 H33 N3 O6
• Title of publication: Synthesis of 3-indolyl all-carbon quaternary centers <i>via</i> Rh/Brønsted acid co-catalyzed three-component reactions of azoalkenes with indoles and diazoacetates.
• Authors of publication: Yue, Xiao-Jing; Pei, Li-Ping; Wang, Min-Can; Jia, Shi-Kun; Mei, Guang-Jian
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2025
• Journal volume: 23
• Journal issue: 22
• Pages of publication: 5323 - 5327
• a: 8.75449 ± 0.00018 Å
• b: 16.6482 ± 0.0004 Å
• c: 19.5357 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2847.26 ± 0.11 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0696
• Residual factor for significantly intense reflections: 0.0601
• Weighted residual factors for significantly intense reflections: 0.1603
• Weighted residual factors for all reflections included in the refinement: 0.1723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No