Information card for entry 7160615

Structure parameters

• Formula: C21 H15 N3 O2
• Calculated formula: C21 H15 N3 O2
• Title of publication: Synthesis of benzo[<i>d</i>,<i>e</i>]quinoline-spiro-succinimides <i>via</i> rhodium-catalyzed C-H activation/annulation of 1-naphthylamides with maleimides.
• Authors of publication: Patel, Raj Naresh; Patel, Dharmik Mahendra; Thakur, Dinesh Gopichand; Rathod, Nileshkumar B.; Patel, Sachinkumar D.; Sonawane, Mahesh A.; Ghosh, Subhash Chandra
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2025
• Journal volume: 23
• Journal issue: 29
• Pages of publication: 6897 - 6902
• a: 8.9088 ± 0.0004 Å
• b: 10.2842 ± 0.0005 Å
• c: 18.4632 ± 0.0008 Å
• α: 90°
• β: 95.65 ± 0.002°
• γ: 90°
• Cell volume: 1683.38 ± 0.13 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0624
• Weighted residual factors for significantly intense reflections: 0.1738
• Weighted residual factors for all reflections included in the refinement: 0.2031
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No