Information card for entry 7160649

Structure parameters

• Chemical name: organic
• Formula: C24 H22 Cl N2 O2 S
• Calculated formula: C24 H21 Cl N2 O2 S
• Title of publication: Diastereoselective synthesis of spiro[cyclopropane-1,3'-indolin]-2'-imines <i>via</i> a sequential [1 + 2] annulation reaction of indolin-2-imines with α-aryl vinylsulfonium salts.
• Authors of publication: Gou, Yan; Hou, Shanling; Fu, Qingyi; Fan, Zhi; Li, Yuming
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2025
• Journal volume: 23
• Journal issue: 32
• Pages of publication: 7415 - 7419
• a: 7.158 ± 0.005 Å
• b: 8.464 ± 0.007 Å
• c: 19.143 ± 0.015 Å
• α: 81.94 ± 0.02°
• β: 79.89 ± 0.02°
• γ: 88.02 ± 0.02°
• Cell volume: 1130.4 ± 1.5 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1555
• Residual factor for significantly intense reflections: 0.0868
• Weighted residual factors for significantly intense reflections: 0.1857
• Weighted residual factors for all reflections included in the refinement: 0.2269
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No