Information card for entry 7160651

Structure parameters

• Formula: C26 H24 N3 O2 S
• Calculated formula: C26 H25 N3 O2 S
• Title of publication: Diastereoselective construction of structurally diverse polycyclic spiroindolenines <i>via</i> Yb(OTf)₃-catalyzed cascade [1,5]-hydride transfer/cyclization.
• Authors of publication: Hu, Song; Hu, Dan; Xu, Jianming; Wang, Jian; Yin, Heng; Xie, Ying; Li, Yulong; Li, Chenyi
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2025
• Journal volume: 23
• Journal issue: 33
• Pages of publication: 7633 - 7637
• a: 12.891 ± 0.0006 Å
• b: 8.2439 ± 0.0003 Å
• c: 21.5146 ± 0.001 Å
• α: 90°
• β: 93.477 ± 0.002°
• γ: 90°
• Cell volume: 2282.19 ± 0.17 ų
• Cell temperature: 273.15 K
• Ambient diffraction temperature: 273.15 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.069
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1511
• Weighted residual factors for all reflections included in the refinement: 0.1636
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No