Information card for entry 7160926

Structure parameters

• Formula: C24 H29 Cl N2 O8
• Calculated formula: C24 H29 Cl N2 O8
• Title of publication: TMEDA-catalyzed synthesis of pentasubstituted 2-aminopyrroles from ynehydrazides and dialkyl acetylenedicarboxylates.
• Authors of publication: Zeng, Zhiwei; Lin, Jingwei; Xie, Yongchao; Guo, Jiangbin; Ma, Nan; Lei, Jian; Lin, Jinguo; Xie, Xiaolan
• Journal of publication: Organic & biomolecular chemistry
• Year of publication: 2026
• Journal volume: 24
• Journal issue: 5
• Pages of publication: 1011 - 1015
• a: 9.8003 ± 0.0005 Å
• b: 11.4521 ± 0.0006 Å
• c: 12.3115 ± 0.0006 Å
• α: 109.781 ± 0.002°
• β: 105.927 ± 0.002°
• γ: 93.616 ± 0.002°
• Cell volume: 1231.62 ± 0.11 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.051
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.1155
• Weighted residual factors for all reflections included in the refinement: 0.1231
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No