Supramolecular assemblies prepared from an iron(II) tripodal complex, tetrafluoroborate, and alkali metal cations. The effect of cation size on coordination number, anion disorder and hydrogen bonding
Authors of publication
Alvarado, Luigi; Brewer, Cynthia; Brewer, Greg; Butcher, Ray J.; Straka, Alison; Viragh, Carol
Journal of publication
CrystEngComm
Year of publication
2009
Journal volume
11
Journal issue
11
Pages of publication
2297
a
9.8471 ± 0.0006 Å
b
22.6507 ± 0.0011 Å
c
12.5484 ± 0.0006 Å
α
90°
β
111.268 ± 0.006°
γ
90°
Cell volume
2608.2 ± 0.3 Å3
Cell temperature
295 ± 2 K
Ambient diffraction temperature
295 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.1763
Residual factor for significantly intense reflections
0.0453
Weighted residual factors for significantly intense reflections
0.1056
Weighted residual factors for all reflections included in the refinement
0.1283
Goodness-of-fit parameter for all reflections included in the refinement
