Information card for entry 7201250

Structure parameters

• Formula: C58 H100 N20 Ni2 O34 Tb2 W2
• Calculated formula: C58 H48 N20 Ni2 O34 Tb2 W2
• Title of publication: 1-D hydrogen-bonded organization of hexanuclear {3d-4f-5d} complexes: evidence for slow relaxation of the magnetization for [{LMe2Ni(H2O)Ln(H2O)4.5}2{W(CN)8}2] with Ln = Tb and Dy
• Authors of publication: Dhers, Sébastien; Sahoo, Shaon; Costes, Jean-Pierre; Duhayon, Carine; Ramasesha, S.; Sutter, Jean-Pascal
• Journal of publication: CrystEngComm
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 10
• Pages of publication: 2078
• a: 18.2699 ± 0.0004 Å
• b: 26.9303 ± 0.0008 Å
• c: 18.3479 ± 0.0005 Å
• α: 90°
• β: 90.658 ± 0.002°
• γ: 90°
• Cell volume: 9026.8 ± 0.4 ų
• Cell temperature: 180 K
• Ambient diffraction temperature: 180 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0903
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for all reflections: 0.0675
• Weighted residual factors for significantly intense reflections: 0.037
• Weighted residual factors for all reflections included in the refinement: 0.037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1194
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No